2-benzenesulfonyl-2,6-cycloheptadienone

Base Information

• Chemical Name: 2-benzenesulfonyl-2,6-cycloheptadienone
• CAS No.: 1092980-15-8
• Molecular Formula: C₁₃H₁₂O₃S
• Molecular Weight: 248.302
• Mol file: 1092980-15-8.mol

Synonyms:2-benzenesulfonyl-2,6-cycloheptadienone

Chemical Property of 2-benzenesulfonyl-2,6-cycloheptadienone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-benzenesulfonyl-2,6-cycloheptadienone

There total 1 articles about 2-benzenesulfonyl-2,6-cycloheptadienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

2-benzenesulfonylmethyl-cyclohex-3-ene-1,2-diol (1092980-09-0) → C13H12O3S (1092980-18-1) + 2-benzenesulfonyl-2,6-cycloheptadienone (1092980-15-8)

Guidance literature:

2-benzenesulfonylmethyl-cyclohex-3-ene-1,2-diol; With silica-supported sodium periodate; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

With silica gel; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1021/jo802064c

Reference yield: 86.0%

2-benzenesulfonyl-2,6-cycloheptadienone (1092980-15-8) → Tropone (539-80-0)

Guidance literature:

With triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 0.583333h; Inert atmosphere;

DOI:10.1021/jo802064c

upstream raw materials:

2-benzenesulfonylmethyl-cyclohex-3-ene-1,2-diol

Downstream raw materials:

Tropone

Refernces