1',3:5,7:9,11:13,15-tetrakis-O-(1-methylethylidene)filipin III

Base Information

• Chemical Name: 1',3:5,7:9,11:13,15-tetrakis-O-(1-methylethylidene)filipin III
• CAS No.: 165329-49-7
• Molecular Formula: C₄₇H₇₄O₁₁
• Molecular Weight: 815.098
• Mol file: 165329-49-7.mol

Synonyms:1',3:5,7:9,11:13,15-tetrakis-O-(1-methylethylidene)filipin III

Chemical Property of 1',3:5,7:9,11:13,15-tetrakis-O-(1-methylethylidene)filipin III

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1',3:5,7:9,11:13,15-tetrakis-O-(1-methylethylidene)filipin III

There total 2 articles about 1',3:5,7:9,11:13,15-tetrakis-O-(1-methylethylidene)filipin III which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetone (67-64-1) + 15-Deoxylagosin (480-49-9) → C44H70O11 + C44H70O11 + 1',3:5,7:9,11:13,15-tetrakis-O-(1-methylethylidene)filipin III (165329-49-7)

Guidance literature:

With pyridinium p-toluenesulfonate; 2,2-dimethoxy-propane; In tetrahydrofuran; Yields of byproduct given. Title compound not separated from byproducts;

Reference yield:

acetic anhydride (108-24-7) + acetone (67-64-1) + 15-Deoxylagosin (480-49-9) → 1',3:5,7:9,11:13,15-tetrakis-O-(1-methylethylidene)filipin III (165329-49-7) + 1',15,26-tris-O-acetyl-3,5:7,9:11,13-tris-O-(1-methylethylidine)filipin III + 1',7,26-tri-O-acetyl-3,5:9,11:13,15-tris-O-(1-methylethylidene)filipin III

Guidance literature:

With dmap; pyridinium p-toluenesulfonate; 2,2-dimethoxy-propane; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, 2.) THF;

upstream raw materials:

acetic anhydride

acetone

15-Deoxylagosin

Refernces