(η6-5-methyl-N-methylindole)(η5-cyclopentadienyl)ruthenium hexafluorophosphate

Base Information

• Chemical Name: (η6-5-methyl-N-methylindole)(η5-cyclopentadienyl)ruthenium hexafluorophosphate
• CAS No.: 112398-46-6
• Molecular Formula: C₁₅H₁₆NRu*F₆P
• Molecular Weight: 456.333
• Mol file: 112398-46-6.mol

Synonyms:(η6-5-methyl-N-methylindole)(η5-cyclopentadienyl)ruthenium hexafluorophosphate

Chemical Property of (η6-5-methyl-N-methylindole)(η5-cyclopentadienyl)ruthenium hexafluorophosphate

Chemical Property:

Purity/Quality:

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Technology Process of (η6-5-methyl-N-methylindole)(η5-cyclopentadienyl)ruthenium hexafluorophosphate

There total 1 articles about (η6-5-methyl-N-methylindole)(η5-cyclopentadienyl)ruthenium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1,5-dimethyl-1H-indole (27816-53-1) + cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate → (η6-5-methyl-N-methylindole)(η5-cyclopentadienyl)ruthenium hexafluorophosphate (112398-46-6)

Guidance literature:

In 1,2-dichloro-ethane; Soln. of 1,5-dimethylindole in 1,2-dichloroethane is degassed with nitrogen, (CpRu(CH3CN)3) is added, at 40-50°C for 15 h under N2.; Solvent is removed, washing (ether (4x)), solid residue is redissolved (acetone), dried (Na2SO4), decolorized (charcoal), concg., ether is added, pptn.; elem. anal.;

upstream raw materials:

1,5-dimethyl-1H-indole

Refernces