acide bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoique

Base Information Edit

Chemical Name:acide bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoique
CAS No.:68048-05-5
Molecular Formula:C₂₂H₁₉ClO₄
Molecular Weight:382.843
Hs Code.:
Mol file:68048-05-5.mol

Synonyms:acide bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoique

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Chemical Property of acide bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoique Edit

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Technology Process of acide bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoique

There total 7 articles about acide bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.8%

: 98968-81-1
bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoate de methyle

: 68048-05-5
acide bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoique

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 85 ℃; for 30h;
DOI:10.1002/hlca.19850680417

Reference yield: 86.0%

: 86191-15-3
ethyl 2,4-di-O-benzyl-5-chloro-orsellinate

: 68048-05-5
acide bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoique

Guidance literature:: With sodium hydroxide; In ethanol; for 18h; Heating;

Reference yield:

: 2524-37-0
ethyl orselinate

: 68048-05-5
acide bis(benzyloxy)-4,6-chloro-3-methyl-2-benzoique

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / sulphuryl chloride / diethyl ether / 1.) room temperature, 1 h, 2.) reflux, 45 min

2: 91 percent / fused potassium carbonate / acetone / 18 h / Heating

3: 86 percent / aq. sodium hydroxide / ethanol / 18 h / Heating

With sodium hydroxide; sulfuryl dichloride; potassium carbonate; In diethyl ether; ethanol; acetone;