Solvent Red 135

Base Information

• Chemical Name: Solvent Red 135
• CAS No.: 20749-68-2
• Deprecated CAS: 59459-26-6,71902-17-5,84420-06-4,71902-17-5
• Molecular Formula: C18H6Cl4N2O
• Molecular Weight: 408.07
• Hs Code.: 3204120000
• European Community (EC) Number: 244-007-9
• UNII: 50TEX4842R
• DSSTox Substance ID: DTXSID6041260
• Nikkaji Number: J225.324K
• Wikidata: Q27260817
• Mol file: 20749-68-2.mol

Synonyms:20749-68-2;Solvent Red 135;8,9,10,11-Tetrachloro-12H-isoindolo[2,1-a]perimidin-12-one;C.I. Solvent Red 135;Solvaperm Red G;Solvent Red 162;12H-Phthaloperin-12-one, 8,9,10,11-tetrachloro-;8,9,10,11-Tetrachloro-12-phthaloperinone;C18H6Cl4N2O;8,9,10,11-Tetrachloro-12H-phthaloperin-12-one;EINECS 244-007-9;C.I. Solvent Red 162;UNII-50TEX4842R;50TEX4842R;8,9,10,11-Tetrachloro-12H-isoindolo-[2,1-a]perimidin-12-one;C.I. 564120;EC 244-007-9;5,6,7,8-tetrachloro-2,11-diazapentacyclo[10.7.1.02,10.04,9.016,20]icosa-1(19),4(9),5,7,10,12,14,16(20),17-nonaen-3-one;DIARESIN RED HS;SOLVENTRED135;Dyes, Solvent Red 135;SCHEMBL332418;DTXSID6041260;C18-H6-Cl4-N2-O;MFCD01791729;AKOS003611390;DS-2802;CI 564120;CS-0010616;A879456;W-110524;12-PHTHALOPERINONE, 8,9,10,11-TETRACHLORO-;Q27260817;5,6,7,8-tetrachloro-2,11-diazapentacyclo[10.7.1.0^{2,10}.0^{4,9}.0^{16,20}]icosa-1(19),4(9),5,7,10,12(20),13,15,17-nonaen-3-one

Chemical Property of Solvent Red 135

Chemical Property:

• Appearance/Colour: COA
• Vapor Pressure: 1.37E-16mmHg at 25°C
• Refractive Index: 1.808
• Boiling Point: 646.3 °C at 760 mmHg
• PKA: 1.85±0.20(Predicted)
• Flash Point: 344.6 °C
• PSA: 34.89000
• Density: 1.77 g/cm³
• LogP: 6.47200
• Storage Temp.: Sealed in dry,Room Temperature
• Water Solubility.: 30μg/L at 20℃
• XLogP3: 5.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 407.920473
• Heavy Atom Count: 25
• Complexity: 628

Purity/Quality:

≥99% ^*data from raw suppliers

8,9,10,11-Tetrachloro-12H-isoindolo-[2,1-a]perimidin-12-one 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC2=C3C(=C1)N=C4C5=C(C(=C(C(=C5Cl)Cl)Cl)Cl)C(=O)N4C3=CC=C2
• Description: Solvent Red 135 is an amino ketone bright red powder that is insoluble in water under normal conditions. It is soluble in chloroform, ethanol, organic solvent, and acetone. It is majorly used as for ABS resin, polystyrene, acetate, polymethyl methacrylate, polyvinyl chloride (PVC) colouring. It is also utilized in polyester fibre protoplasmic colouring. It is used in food packaging and in rubber and plastic rubber.

Technology Process of Solvent Red 135

There total 2 articles about Solvent Red 135 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

→ 8,9,10,11-tetrachloro-isoindolo[2,1-a]perimidin-12-one (20749-68-2)

Guidance literature:

With acetic acid; for 2h; Reflux; Inert atmosphere;

Reference yield:

tetrachlorophthalic anhydride (117-08-8) + 1,4,5,8-naphthalenetetracarboxylic dianhydride (81-30-1) + naphthalene-1,8-diamine (479-27-6) → benzo[lmn]diperimidino[2,1-b:1',2'-j][3,8]phenanthroline-5,8-dione (20749-67-1) + benzo[lmn]diperimidino[2,1-b:2',1'-i][3,8]phenanthroline-7,18-dione (4578-87-4) + 8,9,10,11-tetrachloro-isoindolo[2,1-a]perimidin-12-one (20749-68-2)

Guidance literature:

With 50% by weight of the total weight of vinylpyrrolidine and acrylate; at 110 - 180 ℃; for 1h; Inert atmosphere;

upstream raw materials:

tetrachlorophthalic anhydride

1,4,5,8-naphthalenetetracarboxylic dianhydride

naphthalene-1,8-diamine

Refernces

• 1、 -. "NOVEL COMPOUND, COLORFILTER, AND CHEMOSENSOR FOR DETECTING AMINE-BASED COMPOUND". Paragraph 0073; 0076. . Retrieved 2017/07/23.