N-(diphenylmethyl)-1-phenylethan-1-imine

Base Information

• Chemical Name: N-(diphenylmethyl)-1-phenylethan-1-imine
• CAS No.: 29412-58-6
• Molecular Formula: C₂₁H₁₉N
• Molecular Weight: 285.389
• Mol file: 29412-58-6.mol

Synonyms:N-(diphenylmethyl)-1-phenylethan-1-imine

Chemical Property of N-(diphenylmethyl)-1-phenylethan-1-imine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(diphenylmethyl)-1-phenylethan-1-imine

There total 8 articles about N-(diphenylmethyl)-1-phenylethan-1-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

acetophenone (98-86-2) + Benzhydrylamine (91-00-9) → (E)-1,1-diphenyl-N-(1-phenylethylidene)methanamine (29412-58-6)

Guidance literature:

With magnesium sulfate; In toluene; for 5h; Reflux;

DOI:10.1055/s-0029-1219172

Reference yield: 87.0%

acetophenone (98-86-2) + Benzhydrylamine (91-00-9) → N-(diphenylmethyl)-1-phenylethan-1-imine (29412-58-6)

Guidance literature:

With sodium sulfate; at 135 ℃; for 14h; Inert atmosphere;

DOI:10.1134/S1070428021040138

Reference yield:

benzophenone (119-61-9) → N-(diphenylmethyl)-1-phenylethan-1-imine (29412-58-6)

Guidance literature:

Multi-step reaction with 3 steps

1: formamide; formic acid / 3 h / 190 °C

2: sodium hydroxide / water

3: sodium sulfate / toluene / 90 °C / Reflux

With formic acid; formamide; sodium sulfate; sodium hydroxide; In water; toluene;

DOI:10.3184/174751918X15232662638058

upstream raw materials:

ethanol

1,1-diphenyl-N-(1-phenylethyl)methanimine

sodium ethanolate

benzophenone

Downstream raw materials:

1,1-diphenyl-N-(1-phenylvinyl)methanimine

(R)-N-diphenylmethyl-1-phenylethylamine

1,1-diphenyl-N-(1-phenylethyl)methanimine

1,1-diphenyl-N-[(1R)-1-phenylethyl]methanimine

Refernces

• 1、 -. "METHOD FOR PRODUCING OPTICALLY ACTIVE COMPOUND". Paragraph 0674-0676. . Retrieved 2020/11/27.
• 2、 Sun, Quan-Wei,Xing, Jun-De,Qin, Yu-Hong,Yin, Xu-Wen,Zhou, Yi. "Benzhydrylamine: An effective aminating agent for the synthesis of primary amines". . p. 181 - 183. Retrieved 2018/05/26.