Technology Process of (E)-2-(3,4-dimethoxystyryl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
There total 3 articles about (E)-2-(3,4-dimethoxystyryl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(tBuPNN)CoCl2; sodium triethylborohydride; cesium fluoride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 12h;
stereoselective reaction;
DOI:10.1021/acscatal.7b02104
- Guidance literature:
-
With
Hoveyda-Grubbs catalyst second generation;
In
toluene;
for 1h;
Temperature;
Reagent/catalyst;
Inert atmosphere;
Reflux;
DOI:10.1002/ejoc.201402192
- Guidance literature:
-
With
[1,3-bis(2,4,6-trimethylphenyl)imidazolidin-2-ylidene][2-isopropoxy-5-(2,2,2-trifluoroacetamido)benzylidene]ruthenium(II) dichloride;
In
toluene;
for 1h;
stereoselective reaction;
Inert atmosphere;
Reflux;
DOI:10.1002/ejoc.201402192