Technology Process of diiodobis(1,2-ethylene bis(diphenylphosphine oxide))iron(II)*H2O
There total 1 articles about diiodobis(1,2-ethylene bis(diphenylphosphine oxide))iron(II)*H2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
chloroform; acetone; benzene;
soln. of ligand in chloroform is added to FeI2 soln. in acetone:benzenemixt. and refluxed for 30 min; soln. is concd., petroleum ether (40-60°C) added, solid filtered, dried and recrystd. from CHCl3/acetone/benzene; elem. anal.;
DOI:10.1016/S0277-5387(00)86688-7