phenylimidodiphosphorous tetrachloride

Base Information

• Chemical Name: phenylimidodiphosphorous tetrachloride
• CAS No.: 39652-40-9
• Molecular Formula: C6H5 Cl4 N P2
• Molecular Weight: 294.872
• Mol file: 39652-40-9.mol

Synonyms:Imidodiphosphoroustetrachloride, phenyl- (9CI); N,N-Bis(dichlorophosphino)aniline

Chemical Property of phenylimidodiphosphorous tetrachloride

Chemical Property:

• Vapor Pressure: 0.000355mmHg at 25°C
• Boiling Point: 318.7°Cat760mmHg
• Flash Point: 146.6°C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of phenylimidodiphosphorous tetrachloride

There total 2 articles about phenylimidodiphosphorous tetrachloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aniline hydrochloride (142-04-1,36663-09-9) → N,N'-bis(dichlorophosphino)aniline (39652-40-9)

Guidance literature:

With phosphorus trichloride;

Reference yield:

aniline (62-53-3) → N,N'-bis(dichlorophosphino)aniline (39652-40-9)

Guidance literature:

With phosphorus trichloride;

Reference yield: 95.0%

2,2'-methylenebis(4,6-di-tert-butylphenol) (14362-12-0,38486-51-0) + N,N'-bis(dichlorophosphino)aniline (39652-40-9) → 5,7,15,17-tetra-tert-butyl-10,12-dichloro-11-phenyl-9,13-dioxa-11-aza-10,12-diphospha-tricyclo[12.4.0.03,8]octadeca-1(18),3(8),4,6,14,16-hexaene

Guidance literature:

With triethylamine; In tetrahydrofuran; at -5 - 25 ℃;

DOI:10.1080/10426500307891

upstream raw materials:

aniline hydrochloride

aniline

Downstream raw materials:

N,N,N',N'-Tetramethyl-1,3-diphenyl-[1,3,2,4]diazadiphosphetidine-2,4-diamine

C₆H₅Cl₄NP₂S₂

N,N-Bis(difluorophosphino)anilin

C₆H₅Cl₄NP₂S