PO₂(OH)CF₃^(1-)*C₆H₅NH₃⁽¹⁺⁾=PO(OH)OCF₃C₆H₅NH₃

Base Information

• Chemical Name: PO₂(OH)CF₃^(1-)*C₆H₅NH₃⁽¹⁺⁾=PO(OH)OCF₃C₆H₅NH₃
• CAS No.: 352-86-3
• Molecular Formula: CHF₃O₃P*C₆H₈N
• Molecular Weight: 243.122
• Mol file: 352-86-3.mol

Synonyms:PO₂(OH)CF₃^(1-)*C₆H₅NH₃⁽¹⁺⁾=PO(OH)OCF₃C₆H₅NH₃

Chemical Property of PO₂(OH)CF₃^(1-)*C₆H₅NH₃⁽¹⁺⁾=PO(OH)OCF₃C₆H₅NH₃

Chemical Property:

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Technology Process of PO₂(OH)CF₃^(1-)*C₆H₅NH₃⁽¹⁺⁾=PO(OH)OCF₃C₆H₅NH₃

There total 2 articles about PO₂(OH)CF₃^(1-)*C₆H₅NH₃⁽¹⁺⁾=PO(OH)OCF₃C₆H₅NH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(trifluoromethyl)phosphonic acid (374-09-4) → PO2(OH)CF3(1-)*C6H5NH3(1+)=PO(OH)OCF3C6H5NH3 (352-86-3)

Guidance literature:

With aniline; In ethanol; byproducts: H2O; neutralization at 100°C; acid : base molar ratio = 1 : 1;

Reference yield:

(trifluoromethyl)phosphonic acid (374-09-4) + aniline (62-53-3) → PO3CF3(2-)*2C6H5NH3(1+)=POCF3O2(C6H5NH3)2 + PO2(OH)CF3(1-)*C6H5NH3(1+)=PO(OH)OCF3C6H5NH3 (352-86-3)

Guidance literature:

In ethanol; slow addition of acid to soln. of aniline in ethanol (dissolving via heating to 100°C);; recrystallization of mono-anilinium salt from ethanol, whether mono-aniliunium salt or di-anilinium salt is formed depends on ratio of starting material;;

DOI:10.1039/JR9550000563

upstream raw materials:

(trifluoromethyl)phosphonic acid

aniline