2,6-dibromo-4-butylaniline

Base Information

• Chemical Name: 2,6-dibromo-4-butylaniline
• CAS No.: 10546-66-4
• Molecular Formula: C₁₀H₁₃Br₂N
• Molecular Weight: 307.028
• Mol file: 10546-66-4.mol

Synonyms:2,6-dibromo-4-butylaniline

Chemical Property of 2,6-dibromo-4-butylaniline

Chemical Property:

• Storage Temp.: 2-8°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,6-Dibromo-4-butylaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-dibromo-4-butylaniline

There total 2 articles about 2,6-dibromo-4-butylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-Butylaniline (104-13-2) → 2,6-dibromo-4-butylaniline (10546-66-4)

Guidance literature:

With bromine; In water; at 20 ℃; for 0.166667h;

DOI:10.1021/acs.joc.8b00188

Reference yield:

4-Butylaniline (104-13-2) → 2,6-dibromo-4-butylaniline (10546-66-4) + 2-bromo-4-butylaniline (51605-98-2)

Guidance literature:

With oxygen; copper diacetate; acetic acid; lithium bromide; In dodecane; at 60 ℃; for 3.5h; under 760.051 Torr; chemoselective reaction;

DOI:10.1002/adsc.200800223

Reference yield: 99.0%

2,6-dibromo-4-butylaniline (10546-66-4) + N,N-bis(2-hydroxyethyl)-3-acetamidoaniline (92-02-4) → N-(5-(bis(2-hydroxyethyl)amino)-2-((2,6-dibromo-4-butylphenyl)diazenyl)phenyl)-acetamide (1357264-57-3)

Guidance literature:

2,6-dibromo-4-butylaniline; With acetic acid; propionic acid; at 45 ℃;

With nitrosylsulfuric acid; at 0 - 5 ℃; for 1h;

N,N-bis(2-hydroxyethyl)-3-acetamidoaniline; In water; at 1 - 20 ℃;

upstream raw materials:

4-Butylaniline

Downstream raw materials:

N-(5-(bis(2-hydroxyethyl)amino)-2-((4-butyl-2,6-dicyanophenyl)diazenyl)phenyl)-acetamide

N-(5-(bis(2-hydroxyethyl)amino)-2-((2,6-dibromo-4-butylphenyl)diazenyl)phenyl)-acetamide

Refernces

• 1、 -. "PARTICLES FOR ELECTROPHORETIC DISPLAYS". Page/Page column 97. . Retrieved 2012/03/09.