(E)-2-(3-chloroprop-1-enyl)-1,3,5-trimethoxybenzene

Base Information

• Chemical Name: (E)-2-(3-chloroprop-1-enyl)-1,3,5-trimethoxybenzene
• CAS No.: 1041954-92-0
• Molecular Formula: C₁₂H₁₅ClO₃
• Molecular Weight: 242.702
• Mol file: 1041954-92-0.mol

Synonyms:(E)-2-(3-chloroprop-1-enyl)-1,3,5-trimethoxybenzene

Chemical Property of (E)-2-(3-chloroprop-1-enyl)-1,3,5-trimethoxybenzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (E)-2-(3-chloroprop-1-enyl)-1,3,5-trimethoxybenzene

There total 1 articles about (E)-2-(3-chloroprop-1-enyl)-1,3,5-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-3-(2,4,6-trimethoxyphenyl)prop-2-en-1-ol (100257-91-8) → (E)-2-(3-chloroprop-1-enyl)-1,3,5-trimethoxybenzene (1041954-92-0)

Guidance literature:

With thionyl chloride; In diethyl ether; at 0 ℃;

DOI:10.1002/chem.200702030

Reference yield: 75.0%

(E)-2-(3-chloroprop-1-enyl)-1,3,5-trimethoxybenzene (1041954-92-0) → 1-(2,4,6-trimethoxyphenyl)propan-1-one (834-94-6)

Guidance literature:

With potassium carbonate; phenylboronic acid; [Ru(cyclopentadienyl)(MeCN)3]PF₆; In acetonitrile; at 20 ℃; for 16h;

DOI:10.1039/b801159a

upstream raw materials:

(E)-3-(2,4,6-trimethoxyphenyl)prop-2-en-1-ol

Downstream raw materials:

1-(2,4,6-trimethoxyphenyl)propan-1-one

Refernces