Technology Process of C46H41N3O2S3
There total 7 articles about C46H41N3O2S3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 75 ℃;
for 2h;
microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium phosphate dodecahydrate / palladium 10% on activated carbon / isopropyl alcohol / 4 h / 80 °C
2: acetic acid; N-iodo-succinimide / chloroform
3: sodium phosphate dodecahydrate / palladium 10% on activated carbon / isopropyl alcohol / 24 h / 80 °C
4: pyridine / dichloromethane / 2 h / 75 °C / microwave irradiation
With
pyridine; sodium phosphate dodecahydrate; N-iodo-succinimide; acetic acid;
palladium 10% on activated carbon;
In
dichloromethane; chloroform; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: acetic acid; N-iodo-succinimide / chloroform / 20 °C
2: sodium phosphate dodecahydrate / palladium 10% on activated carbon / isopropyl alcohol / 4 h / 80 °C
3: acetic acid; N-iodo-succinimide / chloroform
4: sodium phosphate dodecahydrate / palladium 10% on activated carbon / isopropyl alcohol / 24 h / 80 °C
5: pyridine / dichloromethane / 2 h / 75 °C / microwave irradiation
With
pyridine; sodium phosphate dodecahydrate; N-iodo-succinimide; acetic acid;
palladium 10% on activated carbon;
In
dichloromethane; chloroform; isopropyl alcohol;