Technology Process of C47H74N4O6
There total 4 articles about C47H74N4O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C43H70N4O4;
dmap;
In
1-methyl-pyrrolidin-2-one; acetonitrile;
Reflux;
acetic anhydride;
In
1-methyl-pyrrolidin-2-one; acetonitrile;
for 6h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / acetic anhydride; toluene / 4 h / 20 - 30 °C
2.1: sodium methylate / ethanol; water; methanol / 5 - 20 °C / Reflux
3.1: acetic acid / 12 h / 20 °C
4.1: dmap / 1-methyl-pyrrolidin-2-one; acetonitrile / Reflux
4.2: 6 h / Reflux
With
pyridine; sodium methylate;
dmap;
In
1-methyl-pyrrolidin-2-one; methanol; ethanol; water; acetic anhydride; acetic acid; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium methylate / ethanol; water; methanol / 5 - 20 °C / Reflux
2.1: acetic acid / 12 h / 20 °C
3.1: dmap / 1-methyl-pyrrolidin-2-one; acetonitrile / Reflux
3.2: 6 h / Reflux
With
sodium methylate;
dmap;
In
1-methyl-pyrrolidin-2-one; methanol; ethanol; water; acetic acid; acetonitrile;