Technology Process of di-n-butyl B-<2-isopropoxy-6-(N,N-diethylcarboxamido)phenyl>boronate
There total 1 articles about di-n-butyl B-<2-isopropoxy-6-(N,N-diethylcarboxamido)phenyl>boronate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium;
In
tetrahydrofuran;
dropwise addn. of a soln. of the benzamide in THF to a stirred soln. of s-BuLi and TMEDA in THF at -78°C; stirring at -78°C for 2 h; addn. of tributyl borate; stirring below -40°C for 4 h; quenching with NH4Cl soln. at -40°C;; short-path distn.; elem. anal.;;
DOI:10.1139/v94-035
