Technology Process of 5-Phenyl-4-pentenoic acid chloride
There total 7 articles about 5-Phenyl-4-pentenoic acid chloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 10percent KOH / methanol; H2O / 2 h / Heating
2: thionyl chloride / 1.5 h / Heating
With
potassium hydroxide; thionyl chloride;
In
methanol; water;
DOI:10.1021/ja00009a041
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) NaOEt
2: 1.) KOH / 1.) EtOH, 2.) heating
3: 1.) 10percent NaOH, 2.) (COCl)2
With
potassium hydroxide; sodium hydroxide; oxalyl dichloride; sodium ethanolate;
DOI:10.1016/S0040-4020(01)87064-2
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 75 percent
2: 75 percent / NaCl / dimethylsulfoxide; H2O / 6 h / Heating
3: 10percent KOH / methanol; H2O / 2 h / Heating
4: thionyl chloride / 1.5 h / Heating
With
potassium hydroxide; thionyl chloride; sodium chloride;
In
methanol; water; dimethyl sulfoxide;
DOI:10.1021/ja00009a041
