C₄₀H₆₂O₁₀Si

Base Information

• Chemical Name: C₄₀H₆₂O₁₀Si
• CAS No.: 1388627-30-2
• Molecular Formula: C₄₀H₆₂O₁₀Si
• Molecular Weight: 731.012
• Mol file: 1388627-30-2.mol

Synonyms:C₄₀H₆₂O₁₀Si

Chemical Property of C₄₀H₆₂O₁₀Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₀H₆₂O₁₀Si

There total 15 articles about C₄₀H₆₂O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(Trimethylsilyl)ethanol (2916-68-9) + C38H54O10 (1388627-49-3) → C40H62O10Si (1388627-30-2)

Guidance literature:

With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃;

DOI:10.1038/nchem.1330

Reference yield:

C14H26O3S2 (1388627-17-5) → C40H62O10Si (1388627-30-2)

Guidance literature:

Multi-step reaction with 10 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -5 °C

2.1: iodine; sodium hydrogencarbonate / water; acetonitrile / -5 °C

3.1: samarium diiodide / tetrahydrofuran; methanol

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

5.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 40 °C

6.1: sodium hydride / 1,2-dimethoxyethane / 0 - 20 °C

7.1: n-butyllithium; 4-Methoxybenzenethiol / 0 - 20 °C

7.2: -78 - 20 °C

8.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C

9.1: ammonium fluoride; tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

10.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

With 1H-imidazole; n-butyllithium; Hoveyda-Grubbs catalyst second generation; samarium diiodide; ammonium fluoride; 4-Methoxybenzenethiol; tetrabutyl ammonium fluoride; iodine; sodium hexamethyldisilazane; sodium hydride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1038/nchem.1330

Reference yield:

C16H30O4S2 (1388627-40-4) → C40H62O10Si (1388627-30-2)

Guidance literature:

Multi-step reaction with 8 steps

1: iodine; sodium hydrogencarbonate / water; acetonitrile / -5 °C

2: samarium diiodide / tetrahydrofuran; methanol

3: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

4: Hoveyda-Grubbs catalyst second generation / dichloromethane / 40 °C

5: sodium hydride / 1,2-dimethoxyethane / 0 - 20 °C

6: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C

7: ammonium fluoride; tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

8: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

With 1H-imidazole; Hoveyda-Grubbs catalyst second generation; samarium diiodide; ammonium fluoride; tetrabutyl ammonium fluoride; iodine; sodium hexamethyldisilazane; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1038/nchem.1330

upstream raw materials:

C₁₄H₂₆O₃S₂

C₁₆H₃₀O₄S₂

C₁₃H₂₄O₅

C₁₃H₂₆O₅

Downstream raw materials:

C₈₁H₁₂₄O₁₉Si₂

Refernces