N N' N -TRIHYDROXYISOCYANURIC ACID

Base Information

• Chemical Name: N N' N -TRIHYDROXYISOCYANURIC ACID
• CAS No.: 143435-52-3
• Molecular Formula: C3H3 N3 O6
• Molecular Weight: 177.073
• Mol file: 143435-52-3.mol

Synonyms:1,3,5-Triazine-2,4,6(1H,3H,5H)-trione,1,3,5-trihydroxy-;1,3,5-Trihydroxyhexahydro-1,3,5-triazine-2,4,6-trione

Chemical Property of N N' N -TRIHYDROXYISOCYANURIC ACID

Chemical Property:

• Melting Point: 240-244 °C (dec.)(lit.)
• Boiling Point: 466.4±28.0 °C(Predicted)
• PKA: 8.29±0.20(Predicted)
• PSA: 126.69000
• Density: 2.946±0.06 g/cm3(Predicted)
• LogP: -3.11640

Purity/Quality:

98%,99%, ^*data from raw suppliers

NN'N-TRIHYDROXYISOCYANURICACID 97% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T
• Statements: 61
• Safety Statements: 53-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N N' N -TRIHYDROXYISOCYANURIC ACID

There total 4 articles about N N' N -TRIHYDROXYISOCYANURIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,3,5-tribenzyloxy-1,3,5-triazine-2,4,6(1H,3H,5H)-trione (95705-20-7) → 1N,3N,5N-trihydroxy-1,3,5-triazin-2,4,6[1H,3H,5H]-trione (143435-52-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In 1,4-dioxane; at 20 ℃; for 3h;

Reference yield:

C27H27N3O9 → 1N,3N,5N-trihydroxy-1,3,5-triazin-2,4,6[1H,3H,5H]-trione (143435-52-3)

Guidance literature:

With hydrogenchloride; In water;

DOI:10.1039/c9ob00216b

Reference yield:

1,3,5-tribenzyl-[1,3,5]triazinane-2,4,6-trione (606-03-1) → 1N,3N,5N-trihydroxy-1,3,5-triazin-2,4,6[1H,3H,5H]-trione (143435-52-3)

Guidance literature:

With palladium on activated charcoal; hydrogen;

DOI:10.1055/s-0033-1338646

upstream raw materials:

1,3,5-tribenzyloxy-1,3,5-triazine-2,4,6(1H,3H,5H)-trione

1,3,5-tribenzyl-[1,3,5]triazinane-2,4,6-trione

Downstream raw materials:

3-acetoxybenzoic acid

4-acetyloxy-benzoic acid

ortho-nitrobenzoic acid

para-chlorobenzoic acid

Refernces

• 1、 Li, Zi-Hao,Fiser, Béla,Jiang, Biao-Lin,Li, Jian-Wei,Xu, Bao-Hua,Zhang, Suo-Jiang. "N -Hydroxyphthalimide/benzoquinone-catalyzed chlorination of hydrocarbon C-H bond using N -chlorosuccinimide". supporting information. p. 3403 - 3408. Retrieved 2019/04/01.
• 2、 Hirai, Naruhisa,Kagayama, Takashi,Tatsukawa, Yoshinobu,Sakaguchi, Satoshi,Ishii, Yasutaka. "Development of an efficient method for preparation of 1,3,5- trihydroxyisocyanuric acid (THICA) and its use as aerobic oxidation catalyst". . p. 8277 - 8280. Retrieved 2007/10/03.