6-AMYL-6-HENDECANOL

Base Information

• Chemical Name: 6-AMYL-6-HENDECANOL
• CAS No.: 5331-63-5
• Molecular Formula: C₁₆H₃₄O
• Molecular Weight: 242.445
• Hs Code.: 2905199090
• Mol file: 5331-63-5.mol

Synonyms:NSC 2309;Tripentylcarbinol; Trispentylcarbinol

Chemical Property of 6-AMYL-6-HENDECANOL

Chemical Property:

• Vapor Pressure: 0.000162mmHg at 25°C
• Boiling Point: 295.1°Cat760mmHg
• PKA: 15.78±0.29(Predicted)
• Flash Point: 130.9°C
• PSA: 20.23000
• Density: 0.835g/cm³
• LogP: 5.45840

Purity/Quality:

99%min ^*data from raw suppliers

TRI-N-AMYL CARBINOL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-AMYL-6-HENDECANOL

There total 9 articles about 6-AMYL-6-HENDECANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

n-pentylmagnesium bromide (693-25-4) + hexanoic acid (142-62-1) → 6-pentyl-undecan-6-ol (5331-63-5)

Guidance literature:

With diethyl ether; zuletzt in Benzol;

DOI:10.1021/ja01211a504

Reference yield:

dipentyl ketone (927-49-1) + n-pentylmagnesium bromide (693-25-4) → 6-pentyl-undecan-6-ol (5331-63-5)

Guidance literature:

Multistep reaction; (i) ether, (ii) aq. HCl;

DOI:10.1021/ja00809a025

Reference yield:

ethyl 3,3-dipentyl-2-oxooctanoate (25594-04-1) → 6-pentyl-undecan-6-ol (5331-63-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / alkaline KMnO₄ / Heating

2: 73 percent Chromat_. / quinoline, O₂, Co(OAc)2*4H₂O / 24 h / 100 °C / var. cat. syst.

With quinoline; alkaline KMNO₄; oxygen; cobalt(II) acetate;

DOI:10.1021/jo00159a038

upstream raw materials:

n-pentylmagnesium bromide

methylammonium carbonate

hexanoic acid

Diethyl carbonate

Downstream raw materials:

6-pentyl-5-undecene

Tri-n-pentylmethyl-Azide

Refernces