Pyridine-2,6-d2

Base Information

• Chemical Name: Pyridine-2,6-d2
• CAS No.: 17265-96-2
• Molecular Formula: C5H3D2N
• Molecular Weight: 81.0855
• Mol file: 17265-96-2.mol

Synonyms:2,6-Dideuteropyridine;

Chemical Property of Pyridine-2,6-d2

Chemical Property:

• Boiling Point: 115.259 °C at 760 mmHg
• Flash Point: 20 °C
• PSA: 12.89000
• Density: 0.981 g/cm³
• LogP: 1.08160

Purity/Quality:

99% ^*data from raw suppliers

Pyridine-2,6-d2 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Pyridine-2,6-d2 (CAS# 17265-96-2) is a useful isotopically labeled research compound.

Technology Process of Pyridine-2,6-d2

There total 1 articles about Pyridine-2,6-d2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Cyanopyridine (100-70-9,1232006-36-8) → 2,6-dideuteropyridine (17265-96-2) + perdeuteriopyridine (7291-22-7)

Guidance literature:

With water-d2; at 260 ℃; for 25h; Yield given; in a sealed glass tube;

Reference yield: 87.0%

2,6-dideuteropyridine (17265-96-2) + C15H12N4O2S → C20H15(2)H2N3O2S

Guidance literature:

With tetrakis(actonitrile)copper(I) hexafluorophosphate; In dichloromethane; at 50 ℃; for 4h;

DOI:10.1021/acs.orglett.0c02333

upstream raw materials:

2-Cyanopyridine

Refernces