C₁₀H₁₁NO₆S

Base Information

• Chemical Name: C₁₀H₁₁NO₆S
• CAS No.: 879148-28-4
• Molecular Formula: C₁₀H₁₁NO₆S
• Molecular Weight: 273.266
• Mol file: 879148-28-4.mol

Synonyms:C₁₀H₁₁NO₆S

Chemical Property of C₁₀H₁₁NO₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C₁₀H₁₁NO₆S

There total 2 articles about C₁₀H₁₁NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

C10H11NO4S (1426841-88-4) → C10H11NO6S (879148-28-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmcl.2012.12.055

Reference yield:

ethyl 4-chloro-3-nitrobenzoate (16588-16-2) → C10H11NO6S (879148-28-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 50 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.bmcl.2012.12.055

Reference yield: 94.0%

C10H11NO6S (879148-28-4) → 4-methylsulfonyl-3-nitro-benzoic acid (81029-08-5)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.bmcl.2012.12.055

upstream raw materials:

ethyl 4-chloro-3-nitrobenzoate

C₁₀H₁₁NO₄S

Downstream raw materials:

C₂₀H₂₅N₃O₆S

C₂₁H₂₃N₃O₆S

C₁₂H₁₄N₂O₇S

C₁₃H₁₆N₂O₇S

Refernces