4,4'-(2-nitro-1,4-phenylene)dimorpholine

Base Information

• Chemical Name: 4,4'-(2-nitro-1,4-phenylene)dimorpholine
• CAS No.: 1259438-49-7
• Molecular Formula: C₁₄H₁₉N₃O₄
• Molecular Weight: 293.323
• Mol file: 1259438-49-7.mol

Synonyms:4,4'-(2-nitro-1,4-phenylene)dimorpholine

Chemical Property of 4,4'-(2-nitro-1,4-phenylene)dimorpholine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4,4'-(2-nitro-1,4-phenylene)dimorpholine

There total 1 articles about 4,4'-(2-nitro-1,4-phenylene)dimorpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

morpholine (110-91-8,99108-56-2) + 4-(4-bromo-2-nitro-phenyl)-morpholine (90841-34-2) → 4,4'-(2-nitro-1,4-phenylene)dimorpholine (1259438-49-7)

Guidance literature:

With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; In toluene; for 2h; Product distribution / selectivity; Reflux;

Reference yield:

4,4'-(2-nitro-1,4-phenylene)dimorpholine (1259438-49-7) → 2,5-dimorpholinoaniline (1018619-15-2)

Guidance literature:

With tin(II) chloride dihdyrate; In ethyl acetate; at 20 ℃; for 1.66667h; Product distribution / selectivity; Reflux;

upstream raw materials:

morpholine

4-(4-bromo-2-nitro-phenyl)-morpholine

Downstream raw materials:

2,5-dimorpholinoaniline

Refernces