(3-phenylpropyl)-[5-(3-phenylpropylamino)pentyl]carbamic acid tert-butyl ester-d2

Base Information

• Chemical Name: (3-phenylpropyl)-[5-(3-phenylpropylamino)pentyl]carbamic acid tert-butyl ester-d2
• CAS No.: 1391748-91-6
• Molecular Formula: C₂₈H₄₂N₂O₂
• Molecular Weight: 440.638
• Mol file: 1391748-91-6.mol

Synonyms:(3-phenylpropyl)-[5-(3-phenylpropylamino)pentyl]carbamic acid tert-butyl ester-d2

Chemical Property of (3-phenylpropyl)-[5-(3-phenylpropylamino)pentyl]carbamic acid tert-butyl ester-d2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3-phenylpropyl)-[5-(3-phenylpropylamino)pentyl]carbamic acid tert-butyl ester-d2

There total 6 articles about (3-phenylpropyl)-[5-(3-phenylpropylamino)pentyl]carbamic acid tert-butyl ester-d2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C28H38(2)H2N2O2 → (3-phenylpropyl)-[5-(3-phenylpropylamino)pentyl]carbamic acid tert-butyl ester-d2 (1391748-91-6)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1002/anie.201200822

Reference yield:

N-(3-phenylpropyl)pentane-1,5-diamine-d2 (1391748-88-1) → (3-phenylpropyl)-[5-(3-phenylpropylamino)pentyl]carbamic acid tert-butyl ester-d2 (1391748-91-6)

Guidance literature:

Multi-step reaction with 4 steps

1: dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

3: water; sodium hydroxide / methanol / 15 h / 20 °C

4: methanol / 72 h / 20 °C / Inert atmosphere

With water; triethylamine; sodium hydroxide; In methanol; dichloromethane;

DOI:10.1002/anie.201200822

Reference yield:

(3-phenylpropyl)-[5-(2,2,2-trifluoroacetylamino)pentyl]carbamic acid tert-butyl ester-d2 (1391748-89-2) → (3-phenylpropyl)-[5-(3-phenylpropylamino)pentyl]carbamic acid tert-butyl ester-d2 (1391748-91-6)

Guidance literature:

Multi-step reaction with 2 steps

1: water; sodium hydroxide / methanol / 15 h / 20 °C

2: methanol / 72 h / 20 °C / Inert atmosphere

With water; sodium hydroxide; In methanol;

DOI:10.1002/anie.201200822

upstream raw materials:

3-phenyl-propionaldehyde

(5-aminopentyl)-(3-phenylpropyl)carbamic acid tert-butyl ester-d2

N-(3-phenylpropyl)pentane-1,5-diamine-d2

(3-phenylpropyl)-[5-(2,2,2-trifluoroacetylamino)pentyl]carbamic acid tert-butyl ester-d2

Downstream raw materials:

N-[2-(4-nitrophenyl)allyl]-N,N'-bis-(3-phenylpropyl)pentane-1,5-diamine-d2

{5-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]pentyl}-(3-phenylpropyl)carbamic acid tert-butyl ester-d2

Refernces