Technology Process of C28H32N2O3
There total 4 articles about C28H32N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
oxalyl dichloride; dimethyl sulfoxide; triethylamine;
In
dichloromethane;
for 1.5h;
DOI:10.1021/ol020170b
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: BH3*THF / 14 h / 0 °C
1.2: 85 percent / hydrogen peroxide / tetrahydrofuran
2.1: 80 percent / oxalyl chloride; dimethyl sulfoxide; triethylamine / CH2Cl2 / 1.5 h
With
borane-THF; oxalyl dichloride; dimethyl sulfoxide; triethylamine;
In
dichloromethane;
2.1: Swern oxidation;
DOI:10.1021/ol020170b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-phenylselenophthalimide; p-toluenesulfonic acid / CH2Cl2; methanol
1.2: 90 percent / sodium metaperiodate / tetrahydrofuran; H2O / 10 h / 0 °C
2.1: BH3*THF / 14 h / 0 °C
2.2: 85 percent / hydrogen peroxide / tetrahydrofuran
3.1: 80 percent / oxalyl chloride; dimethyl sulfoxide; triethylamine / CH2Cl2 / 1.5 h
With
borane-THF; oxalyl dichloride; N-phenylselanylphthalimide; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine;
In
methanol; dichloromethane;
4.1: Swern oxidation;
DOI:10.1021/ol020170b