[2-(4-Chloro-phenyl)-ethyl]-trimethyl-stannane

Base Information

• Chemical Name: [2-(4-Chloro-phenyl)-ethyl]-trimethyl-stannane
• CAS No.: 104586-14-3
• Molecular Formula: C₁₁H₁₇ClSn
• Molecular Weight: 303.419
• Mol file: 104586-14-3.mol

Synonyms:[2-(4-Chloro-phenyl)-ethyl]-trimethyl-stannane

Chemical Property of [2-(4-Chloro-phenyl)-ethyl]-trimethyl-stannane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [2-(4-Chloro-phenyl)-ethyl]-trimethyl-stannane

There total 1 articles about [2-(4-Chloro-phenyl)-ethyl]-trimethyl-stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

1-(2-bromoethyl)-4-chlorobenzene (6529-53-9) + trimethyltin(IV)chloride (1066-45-1) → [2-(4-Chloro-phenyl)-ethyl]-trimethyl-stannane (104586-14-3)

Guidance literature:

With magnesium; In diethyl ether; soln. of (CH3)3SnCl added to Grignard reagent of ClC6H4C2H4Br; purification by fractionation under reduced pressure;

DOI:10.1007/BF00953944

Reference yield: 79.0%

[2-(4-Chloro-phenyl)-ethyl]-trimethyl-stannane (104586-14-3) → 4-vinylbenzyl chloride (1073-67-2,24991-47-7)

Guidance literature:

With tris(4-methylphenyl)methylium tetrafluoroborate; In 1,2-dichloro-ethane; at 20 ℃;

DOI:10.1007/BF00953944

upstream raw materials:

1-(2-bromoethyl)-4-chlorobenzene

trimethyltin(IV)chloride

Downstream raw materials:

4-vinylbenzyl chloride

Refernces