2,3-DIIODONAPHTHALENE

Base Information

• Chemical Name: 2,3-DIIODONAPHTHALENE
• CAS No.: 27715-43-1
• Molecular Formula: C10H6 I2
• Molecular Weight: 379.967
• Mol file: 27715-43-1.mol

Synonyms:2,3-Diiodonaphthalene

Chemical Property of 2,3-DIIODONAPHTHALENE

Chemical Property:

• PSA: 0.00000
• LogP: 4.04900

Purity/Quality:

98%min ^*data from raw suppliers

2,3-Diiodonaphthalene 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-DIIODONAPHTHALENE

There total 11 articles about 2,3-DIIODONAPHTHALENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,3-Diaminonaphthalene (771-97-1) → 2,3-diiodonaphthalene (27715-43-1)

Guidance literature:

With potassium iodide; sodium nitrite; In acetic acid;

DOI:10.1021/jp0219202

Reference yield: 83.0%

C20H6Cl12I2 → 2,3-diiodonaphthalene (27715-43-1)

Guidance literature:

at 210 ℃; under 0.007501 - 0.011251 Torr; sublimation;

DOI:10.1081/SCC-120021997

Reference yield: 69.0%

2-(trimethylsilyl)naphthalen-3-yl trifluoromethanesulfonate (780820-43-1) → 2,3-diiodonaphthalene (27715-43-1)

Guidance literature:

With iodine; cesium fluoride; In acetonitrile; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1021/ol300439r

upstream raw materials:

2-Amino-3-naphthoic acid

1,2-bis(iodoethynyl)benzene

2,3-Diaminonaphthalene

1,2-diethynylbenzene

Downstream raw materials:

dimethyl 1,4-dimethyl-7,14-diphenylindeno[1,2,3-cd]naphtho[2,3-k]fluoranthene-2,3-dicarboxylate

1,2-dihydro-5,12-diphenylcyclopenta[cd]naphtho[2,3-k]fluoranthene

2-phenyl-1H-benzo[f]isoindole-1,3(2H)-dione

Refernces

• 1、 -. "A method for preparing isothiaurea compounds based on substituted iodobenzene". Paragraph 0018. . Retrieved 2021/12/07.
• 2、 Nobusue, Shunpei,Mukai, Yuichi,Fukumoto, Yo,Umeda, Rui,Tahara, Kazukuni,Sonoda, Motohiro,Tobe, Yoshito. "Molecular propellers that consist of dehydrobenzo[14]annulene blades". supporting information. p. 12814 - 12824,11. Retrieved 2020/09/14.