α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril

Base Information

• Chemical Name: α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril
• CAS No.: 93148-41-5
• Molecular Formula: C₁₆H₂₃NO₂
• Molecular Weight: 261.364
• Mol file: 93148-41-5.mol

Synonyms:α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril

Chemical Property of α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril

There total 2 articles about α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3,4-dimethoxyphenylacetonitrile (93-17-4) + hexan-1-ol (111-27-3) → α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril (93148-41-5)

Guidance literature:

With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate; In toluene; at 135 ℃; for 4h; Inert atmosphere;

DOI:10.1021/acscatal.7b01427

Reference yield:

→ α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril (93148-41-5)

Guidance literature:

Verb. /BRN= 670110/)(nicht beschr.), aethanol. KOH, Kochen;

DOI:10.1002/hlca.19630460646

upstream raw materials:

3,4-dimethoxyphenylacetonitrile

hexan-1-ol

Refernces