ethyl 3-(dimethylamino)phenyl carbonate

Base Information

• Chemical Name: ethyl 3-(dimethylamino)phenyl carbonate
• CAS No.: 739315-54-9
• Molecular Formula: C₁₁H₁₅NO₃
• Molecular Weight: 209.245
• Mol file: 739315-54-9.mol

Synonyms:ethyl 3-(dimethylamino)phenyl carbonate

Chemical Property of ethyl 3-(dimethylamino)phenyl carbonate

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of ethyl 3-(dimethylamino)phenyl carbonate

There total 2 articles about ethyl 3-(dimethylamino)phenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

diethyl dicarbonate (1609-47-8) + 3-Dimethylaminophenol (99-07-0) → ethyl 3-(dimethylamino)phenyl carbonate (739315-54-9)

Guidance literature:

With magnesium(II) perchlorate; at 40 ℃; for 4.5h;

DOI:10.1002/ejoc.200600366

Reference yield:

chloroformic acid ethyl ester (541-41-3) + 3-Dimethylaminophenol (99-07-0) → ethyl 3-(dimethylamino)phenyl carbonate (739315-54-9)

Guidance literature:

With sodium hydroxide;

DOI:10.1039/jr9340000651

Reference yield:

ethyl 3-(dimethylamino)phenyl carbonate (739315-54-9) → 3-(2-ethoxycarbonyloxy-4-dimethylamino-phenyl)-3-(4-dimethylamino-2-hydroxy-phenyl)-3H-benz[de]isochromen-1-one

Guidance literature:

Multi-step reaction with 2 steps

1: aluminium chloride; 1,1,2,2-tetrachloro-ethane

2: barium hydroxide; methanol / Erwaermen der Reaktionsloesung mit wss. Schwefelsaeure

With methanol; barium dihydroxide; aluminium trichloride; 1,1,2,2-tetrachloroethane;

DOI:10.1039/jr9340000651

upstream raw materials:

chloroformic acid ethyl ester

3-Dimethylaminophenol

diethyl dicarbonate

Refernces