2-(2'-BROMOPHENOXY)PROPANE

Base Information

• Chemical Name: 2-(2'-BROMOPHENOXY)PROPANE
• CAS No.: 701-07-5
• Molecular Formula: C9H11BrO
• Molecular Weight: 215.09
• Hs Code.: 2909309090
• Mol file: 701-07-5.mol

Synonyms:Ether,o-bromophenyl isopropyl (6CI,7CI,8CI);1-Bromo-2-(1-methylethoxy)benzene;1-Bromo-2-isopropoxybenzene;2-Bromo-1-isopropoxybenzene;2-Isopropoxyphenylbromide;o-Isopropoxyphenyl bromide;

Chemical Property of 2-(2'-BROMOPHENOXY)PROPANE

Chemical Property:

• Vapor Pressure: 0.0837mmHg at 25°C
• Refractive Index: 1.523
• Boiling Point: 288.4 °C at 760 mmHg
• Flash Point: 128.2 °C
• PSA: 9.23000
• Density: 1.446 g/cm³
• LogP: 3.23630
• Storage Temp.: Sealed in dry,Room Temperature
• Water Solubility.: Slightly soluble in water.

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-(2''-Bromophenoxy)propane ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 1-Bromo-2-isopropoxybenzene is used as an intermediate in organic syntheses.

Technology Process of 2-(2'-BROMOPHENOXY)PROPANE

There total 7 articles about 2-(2'-BROMOPHENOXY)PROPANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-hydroxybromobenzene (95-56-7) + isopropyl bromide (75-26-3) → 1-bromo-2-isopropoxybenzene (701-07-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 65 ℃; for 4h;

DOI:10.1021/jo0012849

Reference yield:

2-iodo-propane (75-30-9) + 2-hydroxybromobenzene (95-56-7) → 1-bromo-2-isopropoxybenzene (701-07-5)

Guidance literature:

With sodium; potassium carbonate; In diethyl ether; isopropyl alcohol;

Reference yield:

2-hydroxybromobenzene (95-56-7) → 1-bromo-2-isopropoxybenzene (701-07-5)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 8h;

DOI:10.1016/j.bmcl.2007.04.098

upstream raw materials:

propene

2-hydroxybromobenzene

isopropyl bromide

2-iodo-propane

Downstream raw materials:

2-(1-methylethoxy)phenyl-1-piperazine

C₁₉H₂₉NO₄

2-isopropoxyphenylboronic acid

2-isopropoxybenzoic acid

Refernces

• 1、 Simonetti, Sebastian O.,Larghi, Enrique L.,Kaufman, Teodoro S.. "Alternate and step-economic synthesis of the β-Methylstyrene chelating pre-ligand of the Hoveyda-Grubbs II catalyst". . p. 227 - 231. Retrieved 2015/05/27.
• 2、 -. "PYRROLOPYRIMIDINE ALKYNYL COMPOUNDS AND METHODS OF MAKING AND USING SAME". Page/Page column 59. . Retrieved 2009/05/30.