Technology Process of Carbonic acid 4-heptadecyl-[1,3]dioxolan-2-ylmethyl ester phenyl ester
There total 4 articles about Carbonic acid 4-heptadecyl-[1,3]dioxolan-2-ylmethyl ester phenyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / 70percent aq. tert-butyl hydroperoxide (TBHP), 0.02 M OsO4 / acetone; 2-methyl-propan-2-ol / 1.) 0 deg C, 1 h, 2.) RT, 48 h
2: camphorsulfonyl acid (CSA) / toluene / 18 h
3: H2 / 5percent Pd/C / CH2Cl2; ethanol / 18 h / 5171.5 Torr / Ambient temperature
4: pyridine / CH2Cl2 / 1 h / 0 °C
With
pyridine; tert.-butylhydroperoxide; osmium(VIII) oxide; camphor-10-sulfonic acid; hydrogen;
palladium on activated charcoal;
In
ethanol; dichloromethane; acetone; toluene; tert-butyl alcohol;
DOI:10.1021/jm00105a058
- Guidance literature:
-
Multi-step reaction with 3 steps
1: camphorsulfonyl acid (CSA) / toluene / 18 h
2: H2 / 5percent Pd/C / CH2Cl2; ethanol / 18 h / 5171.5 Torr / Ambient temperature
3: pyridine / CH2Cl2 / 1 h / 0 °C
With
pyridine; camphor-10-sulfonic acid; hydrogen;
palladium on activated charcoal;
In
ethanol; dichloromethane; toluene;
DOI:10.1021/jm00105a058
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2 / 5percent Pd/C / CH2Cl2; ethanol / 18 h / 5171.5 Torr / Ambient temperature
2: pyridine / CH2Cl2 / 1 h / 0 °C
With
pyridine; hydrogen;
palladium on activated charcoal;
In
ethanol; dichloromethane;
DOI:10.1021/jm00105a058
