Adenosine, uridylyl-(3'®5')-adenylyl-(3'®5')- (7CI,8CI,9CI)

Base Information

• Chemical Name: Adenosine, uridylyl-(3'®5')-adenylyl-(3'®5')- (7CI,8CI,9CI)
• CAS No.: 2889-33-0
• Molecular Formula: C29H36 N12 O18 P2
• Molecular Weight: 902.622
• Mol file: 2889-33-0.mol

Synonyms:Uridine,adenylyl-(5'®3')-adenylyl-(5'®3')- (8CI); U-A-A

Chemical Property of Adenosine, uridylyl-(3'®5')-adenylyl-(3'®5')- (7CI,8CI,9CI)

Chemical Property:

• PSA: 454.34000
• LogP: -2.91200

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Adenosine, uridylyl-(3'®5')-adenylyl-(3'®5')- (7CI,8CI,9CI)

There total 2 articles about Adenosine, uridylyl-(3'®5')-adenylyl-(3'®5')- (7CI,8CI,9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5'-adenosine monophosphate (61-19-8,24937-83-5,67583-85-1) → D,D,D-U(3'-5')pA(3'-5')pA (2889-33-0) + phosphoric acid adenosin-5'-yl ester uridin-3'-yl ester (3256-24-4) + D,D-U(2'-5')pA (10453-52-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 2,2'-dipyridyldisulphide; triethylamine; triphenylphosphine / dimethyl sulfoxide; N,N-dimethyl-formamide / 3 h

1.2: 2 h

2.1: Na(+)-montmorillonite / 1 h / 24 °C

2.2: 24 °C

With 2,2'-dipyridyldisulphide; triethylamine; triphenylphosphine; In dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1080/15257770.2012.701787

Reference yield:

adenosine 5'-phosphoroimidazolidate sodium salt (60031-83-6) + uridine (58-96-8) → D,D,D-U(3'-5')pA(3'-5')pA (2889-33-0) + phosphoric acid adenosin-5'-yl ester uridin-3'-yl ester (3256-24-4) + D,D-U(2'-5')pA (10453-52-8)

Guidance literature:

uridine; With Na(+)-montmorillonite; at 24 ℃; for 1h;

adenosine 5'-phosphoroimidazolidate sodium salt; at 24 ℃;

DOI:10.1080/15257770.2012.701787

upstream raw materials:

5'-adenosine monophosphate

adenosine 5'-phosphoroimidazolidate sodium salt

uridine

Refernces