4-nitrophenyl sulfurochloridate

Base Information

• Chemical Name: 4-nitrophenyl sulfurochloridate
• CAS No.: 18997-12-1
• Molecular Formula: C₆H₄ClNO₅S
• Molecular Weight: 237.62
• Mol file: 18997-12-1.mol

Synonyms:4-nitrophenyl sulfurochloridate

Chemical Property of 4-nitrophenyl sulfurochloridate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-nitrophenyl sulfurochloridate

There total 2 articles about 4-nitrophenyl sulfurochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(4-nitrophenoxy)butanoic acid (28341-54-0) → 4-nitrophenyl sulfurochloridate (18997-12-1)

Guidance literature:

With sulfuryl dichloride; toluene;

Reference yield:

→ 4-nitrophenyl sulfurochloridate (18997-12-1)

Guidance literature:

p-Nitrophenol;

DOI:10.1139/v72-306

Reference yield: 88.0%

4-nitrophenyl sulfurochloridate (18997-12-1) + C38H36N6O5 → C44H39N7O10S

Guidance literature:

C₃₈H₃₆N₆O₅; With 4-nitro-phenol; triethylamine; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

4-nitrophenyl sulfurochloridate; In dichloromethane; at -78 - 20 ℃; Molecular sieve;

upstream raw materials:

4-(4-nitrophenoxy)butanoic acid

Downstream raw materials:

sulfuric acid bis-(4-nitro-phenyl ester)

4-nitrophenyl phenyl sulfate

sulfuric acid 4-nitrophenyl ester 2,2,2-trichloroethyl ester

2-benzyloxycarbonylphenyl 4-nitrophenyl sulphate