Technology Process of C24H39O8P
There total 7 articles about C24H39O8P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
rhodium (II) octanoate dimer;
In
dichloromethane;
at 85 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1021/ol3017676
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 1.5 h / -78 °C
2: rhodium (II) octanoate dimer / dichloromethane / 1.5 h / 85 °C / Inert atmosphere
With
rhodium (II) octanoate dimer; diisobutylaluminium hydride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ol3017676
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 °C
1.2: 18.5 h / 0 - 20 °C
2.1: Dess-Martin periodane / dichloromethane / 20 °C / Cooling with ice
3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 19 h / 0 - 20 °C
4.1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 1.5 h / -78 °C
5.1: rhodium (II) octanoate dimer / dichloromethane / 1.5 h / 85 °C / Inert atmosphere
With
rhodium (II) octanoate dimer; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil;
DOI:10.1021/ol3017676