(2E)-3-(3,4-dimethoxyphenyl)-2-propenamide

Base Information Edit

Chemical Name:(2E)-3-(3,4-dimethoxyphenyl)-2-propenamide
CAS No.:130973-10-3
Molecular Formula:C₁₁H₁₃NO₃
Molecular Weight:207.229
Hs Code.:
Mol file:130973-10-3.mol

Synonyms:(2E)-3-(3,4-dimethoxyphenyl)-2-propenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E)-3-(3,4-dimethoxyphenyl)-2-propenamide Edit

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Technology Process of (2E)-3-(3,4-dimethoxyphenyl)-2-propenamide

There total 3 articles about (2E)-3-(3,4-dimethoxyphenyl)-2-propenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1597410-34-8
(E)-S-methyl 4-(3,4-dimethoxyphenyl)-2-oxobut-3-enethioate

: 130973-10-3
(2E)-3-(3,4-dimethoxyphenyl)-2-propenamide

Guidance literature:: With diphenylphosphoranyl azide; copper(II) bis(trifluoromethanesulfonate); In water; N,N-dimethyl-formamide; at 100 ℃; for 3.5h;
DOI:10.1021/acs.joc.7b03054

Reference yield: 78.0%

: 2859-78-1
4-Bromoveratrole

: 79-06-1,12624-24-7,25038-45-3,27754-57-0,33338-03-3,39387-77-4,68247-81-4,9082-06-8,79079-15-5
2-propenamide

: 130973-10-3
(2E)-3-(3,4-dimethoxyphenyl)-2-propenamide

Guidance literature:: With palladium diacetate; sodium acetate trihydrate; Tri(p-tolyl)phosphine; In N,N-dimethyl-formamide; at 140 ℃; for 0.333333h; Schlenk technique; Inert atmosphere; Darkness; Sealed tube;
DOI:10.1002/chem.201502968

Reference yield: 36.0%

: 14737-89-4
3,4-dimethoxy-trans-cinnamic acid

: 130973-10-3
(2E)-3-(3,4-dimethoxyphenyl)-2-propenamide

Guidance literature:: 3,4-dimethoxy-trans-cinnamic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

With ammonium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 18.3333h;
DOI:10.1039/b810855b