2-ethoxy-6-phenylnapthalene

Base Information

• Chemical Name: 2-ethoxy-6-phenylnapthalene
• CAS No.: 858458-42-1
• Molecular Formula: C₁₈H₁₆O
• Molecular Weight: 248.324
• Mol file: 858458-42-1.mol

Synonyms:2-ethoxy-6-phenylnapthalene

Chemical Property of 2-ethoxy-6-phenylnapthalene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-ethoxy-6-phenylnapthalene

There total 4 articles about 2-ethoxy-6-phenylnapthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-ethoxy-6-bromo-naphthalene (66217-19-4) + phenylboronic acid (98-80-6) → 2-ethoxy-6-phenylnapthalene (858458-42-1)

Guidance literature:

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; In toluene; at 80 ℃; for 24h; Inert atmosphere;

DOI:10.1002/anie.201201153

Reference yield:

ethyl-(6-cyclohex-1-enyl-[2]naphthyl)-ether → 2-ethoxy-6-phenylnapthalene (858458-42-1)

Guidance literature:

With chloranil; xylene;

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → 2-ethoxy-6-phenylnapthalene (858458-42-1)

Guidance literature:

Multi-step reaction with 2 steps

1: anschliessendes Erhitzen in Xylol mit wenig Jod

2: tetrachloro-<1,4>benzoquinone; xylene

With chloranil; xylene;

upstream raw materials:

2-ethoxynaphthalene

benzene

cyclohexanone

2-ethoxy-6-bromo-naphthalene

Downstream raw materials:

2-phenylnaphthalene

Refernces