N-benzyl-N-methyl-L-histidine methyl ester

Base Information Edit

Chemical Name:N-benzyl-N-methyl-L-histidine methyl ester
CAS No.:866392-18-9
Molecular Formula:C₁₅H₁₉N₃O₂
Molecular Weight:273.335
Hs Code.:
Mol file:866392-18-9.mol

Synonyms:N-benzyl-N-methyl-L-histidine methyl ester

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Chemical Property of N-benzyl-N-methyl-L-histidine methyl ester Edit

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Technology Process of N-benzyl-N-methyl-L-histidine methyl ester

There total 8 articles about N-benzyl-N-methyl-L-histidine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69937-81-1
2-benzylamino-3-(3H-imidazol-4-yl)-propionic acid methyl ester

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 866392-18-9
N-benzyl-N-methyl-L-histidine methyl ester

Guidance literature:: 2-benzylamino-3-(3H-imidazol-4-yl)-propionic acid methyl ester; formaldehyd; In methanol; at 20 ℃; for 5h;

With sodium cyanoborohydride; In methanol; at 20 ℃; for 18h;
DOI:10.1021/ol051441w

Reference yield:

: 78640-70-7
C₁₄H₁₅N₃O₂

: 866392-18-9
(S)-methyl 2-(benzyl(methyl)amino)-3-(1H-imidazol-4-yl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaBH₃CN / methanol / 18 h

2.1: methanol / 5 h

2.2: 554 mg / NaBH₃CN / methanol / 18 h

With sodium cyanoborohydride; In methanol;
DOI:10.1039/b703835f

Reference yield:

: 100-52-7
benzaldehyde

: 866392-18-9
(S)-methyl 2-(benzyl(methyl)amino)-3-(1H-imidazol-4-yl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / 1 h

2.1: NaBH₃CN / methanol / 18 h

3.1: methanol / 5 h

3.2: 554 mg / NaBH₃CN / methanol / 18 h

With sodium cyanoborohydride; In methanol;
DOI:10.1039/b703835f