m-methylphenylphenylmethanol acetate

Base Information

• Chemical Name: m-methylphenylphenylmethanol acetate
• CAS No.: 1438894-51-9
• Molecular Formula: C₁₆H₁₆O₂
• Molecular Weight: 240.302
• Mol file: 1438894-51-9.mol

Synonyms:m-methylphenylphenylmethanol acetate

Chemical Property of m-methylphenylphenylmethanol acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of m-methylphenylphenylmethanol acetate

There total 1 articles about m-methylphenylphenylmethanol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-methyl-3-(phenylmethyl)-benzene (620-47-3) + acetic acid (64-19-7,77671-22-8) → m-methylphenylphenylmethanol acetate (1438894-51-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,2-dichloro-ethane; at 100 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1002/cssc.201200458

Reference yield: 97.0%

m-methylphenylphenylmethanol acetate (1438894-51-9) → 3-methyl benzophenone (643-65-2)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In water; chlorobenzene; at 130 ℃; for 2h;

upstream raw materials:

1-methyl-3-(phenylmethyl)-benzene

acetic acid

Downstream raw materials:

3-methyl benzophenone

Refernces

• 1、 Yi, Hong,Liu, Qiang,Liu, Jie,Zeng, Ziqi,Yang, Yuhong,Lei, Aiwen. "DDQ-catalyzed oxidative C-O coupling of sp3 C-H bonds with carboxylic acids". . p. 2143 - 2146. Retrieved 2013/01/15.