2-(4-AMINOPHENYL)ETHYL AMINE 2HCL

Base Information

• Chemical Name: 2-(4-AMINOPHENYL)ETHYL AMINE 2HCL
• CAS No.: 13078-82-5
• Molecular Formula: C₈H₁₂N₂*2ClH
• Molecular Weight: 209.119
• Hs Code.: 29214990
• Mol file: 13078-82-5.mol

Synonyms:Phenethylamine, p-amino-, dihydrochloride(7CI,8CI);4-(2-Aminoethyl)aniline dihydrochloride;Benzeneethanamine,4-amino-, dihydrochloride (9CI);4-Aminophenethylamine dihydrochloride;4-Aminobenzeneethanaminedihydrochloride;

Chemical Property of 2-(4-AMINOPHENYL)ETHYL AMINE 2HCL

Chemical Property:

• Vapor Pressure: 0.000537mmHg at 25°C
• Melting Point: 296 °C (decomp)
• Boiling Point: 307.5°C at 760 mmHg
• Flash Point: 139.7°C
• PSA: 52.04000
• LogP: 2.85350

Purity/Quality:

99% ^*data from raw suppliers

2-(4-Aminophenyl)ethylamineDihydrochloride ^*data from reagent suppliers

Safty Information:

• Statements: 34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-(4-Aminophenyl)ethylamine Dihydrochloride is used in the preparation of Tyrosol and its transformation into Hordenine.

Technology Process of 2-(4-AMINOPHENYL)ETHYL AMINE 2HCL

There total 2 articles about 2-(4-AMINOPHENYL)ETHYL AMINE 2HCL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-amino-L-phenylalanine (943-80-6) → 4-(2-aminoethyl)aniline dihydrochloride (13078-82-5,29968-79-4,102606-30-4)

Guidance literature:

4-amino-L-phenylalanine; With (R)-Carvone; In propan-1-ol; at 0 - 190 ℃; Green chemistry;

With hydrogenchloride; In propan-1-ol; water; at 190 ℃; for 0.133333h; Microwave irradiation; Green chemistry;

DOI:10.1080/00397911.2015.1100745

Reference yield:

→ 4-(2-aminoethyl)aniline dihydrochloride (13078-82-5,29968-79-4,102606-30-4)

Guidance literature:

Reference yield: 97.0%

2-[4-([3-tert-butoxycarobnylaminophenyl]amino)-6-[2-[4-[4-([3-tert-butoxycarbonylaminophenyl]amino)-6-chloro[1,3,5]triazine-2-ylamino]phenyl]ethylamino][1,3,5]triazine-2-ylamino]ethanol (1192801-08-3) + 4-(2-aminoethyl)aniline dihydrochloride (13078-82-5,29968-79-4,102606-30-4) → 2-(4-(4-(4-(4-aminophenethylamino)-6-(3-(tert-butoxycarbonylamino)phenylamino)-1,3,5-triazin-2-ylamino)phenylethylamino)-6-(3-(tert-butoxycarbonylamino)phenylamino)-1,3,5-triazin-2-ylamino)ethanol (1192801-09-4)

Guidance literature:

With triethylamine; In water; acetonitrile; at 60 ℃; for 24h; Large scale reaction;

DOI:10.1021/op900202b

upstream raw materials:

4-amino-L-phenylalanine

Downstream raw materials:

2-(4-(4-(4-(4-aminophenethylamino)-6-(3-(tert-butoxycarbonylamino)phenylamino)-1,3,5-triazin-2-ylamino)phenylethylamino)-6-(3-(tert-butoxycarbonylamino)phenylamino)-1,3,5-triazin-2-ylamino)ethanol

2-[4-[2-[4-aminophenyl]ethylamino]-6-([3-tert-butoxycarbonylaminophenyl]amino)[1,3,5]triazine-2-ylamino]ethanol

Refernces

• 1、 -. "FRICTIONLESS MOLECULAR ROTARY MOTORS". Page/Page column 33. . Retrieved 2010/02/17.