acetylthiomethyl methyl sulphoxide

Base Information

• Chemical Name: acetylthiomethyl methyl sulphoxide
• CAS No.: 73975-52-7
• Molecular Formula: C₄H₈O₂S₂
• Molecular Weight: 152.238
• Mol file: 73975-52-7.mol

Synonyms:acetylthiomethyl methyl sulphoxide

Chemical Property of acetylthiomethyl methyl sulphoxide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of acetylthiomethyl methyl sulphoxide

There total 1 articles about acetylthiomethyl methyl sulphoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

S-methyl methanethiosulfinate (13882-12-7) + acetic anhydride (108-24-7) → methanethiosulfonic acid S-methyl ester (2949-92-0,31761-75-8) + Dimethyldisulphide (624-92-0) + 2,3,5-trithiahexane 5-oxide (42474-27-1) + acetylthiomethyl methyl sulphoxide (73975-52-7)

Guidance literature:

With acetic acid; at 90 ℃; for 2h;

DOI:10.1039/P29800000432

Reference yield: 42.0%

p-nitrobenzyl (5R,6S)-6-[(R)-1-t-butyldimethylsilyloxy]ethyl-2-ethylsulfinyl-thio-2-penem-3-carboxylate + acetylthiomethyl methyl sulphoxide (73975-52-7) → p-Nitrobenzyl (5R,6S)-6-[(R)-1-t-Butyldimethylsilyloxymethyl]-2-methylsulfinylmethylthio-2-penem-3-carboxylate

Guidance literature:

With sodium methylate; acetic acid; In tetrahydrofuran; ethyl acetate;

upstream raw materials:

S-methyl methanethiosulfinate

acetic anhydride

Refernces