C₂₈H₂₆N₄S₂

Base Information

• Chemical Name: C₂₈H₂₆N₄S₂
• CAS No.: 1613643-11-0
• Molecular Formula: C₂₈H₂₆N₄S₂
• Molecular Weight: 482.673
• Mol file: 1613643-11-0.mol

Synonyms:C₂₈H₂₆N₄S₂

Chemical Property of C₂₈H₂₆N₄S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₂₆N₄S₂

There total 3 articles about C₂₈H₂₆N₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-di(thiazol-2-yl)benzene (13816-22-3) + tert-butyl-(3-iodophenylethyl)carbamate (1613642-60-6) → C28H26N4S2 (1613643-11-0)

Guidance literature:

1,3-di(thiazol-2-yl)benzene; tert-butyl-(3-iodophenylethyl)carbamate; With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triphenylphosphine; silver carbonate; In water; at 60 ℃;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

(3-iodophenyl)acetonitrile (130723-54-5) → C28H26N4S2 (1613643-11-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron trifluoride-tetrahydrofuran complex / tetrahydrofuran / 0 °C / Reflux

1.2: 4 h / 20 °C

2.1: silver carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triphenylphosphine / water / 60 °C

2.2: 4 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; boron trifluoride-tetrahydrofuran complex; triphenylphosphine; silver carbonate; In tetrahydrofuran; water;

Reference yield:

1,3-benzenedicarboxylic acid dithioamide (3030-54-4) → C28H26N4S2 (1613643-11-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethanol / Reflux

2.1: silver carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triphenylphosphine / water / 60 °C

2.2: 4 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triphenylphosphine; silver carbonate; In ethanol; water;

upstream raw materials:

1,3-di(thiazol-2-yl)benzene

tert-butyl-(3-iodophenylethyl)carbamate

(3-iodophenyl)acetonitrile

1,3-benzenedicarboxylic acid dithioamide

Refernces