N^ε-(Boc, methyl)-L-lysine-MCA

Base Information

• Chemical Name: N^ε-(Boc, methyl)-L-lysine-MCA
• CAS No.: 1598424-87-3
• Molecular Formula: C₂₂H₃₁N₃O₅
• Molecular Weight: 417.505
• Mol file: 1598424-87-3.mol

Synonyms:N^ε-(Boc, methyl)-L-lysine-MCA

Chemical Property of N^ε-(Boc, methyl)-L-lysine-MCA

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N^ε-(Boc, methyl)-L-lysine-MCA

There total 1 articles about N^ε-(Boc, methyl)-L-lysine-MCA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Νε-tert-butoxycarbonyl-Να-(9-fluorenylmethoxycarbonyl)-Νε-methyllysine (951695-85-5,2044709-77-3) → Nε-(Boc, methyl)-L-lysine-MCA (1598424-87-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 1 h / Cooling with ice

1.2: 20 °C

2.1: piperidine / N,N-dimethyl-formamide / 0.5 h / 20 °C

With piperidine; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1007/s00726-014-1690-6

upstream raw materials:

Ν_ε-tert-butoxycarbonyl-Ν_α-(9-fluorenylmethoxycarbonyl)-Ν_ε-methyllysine

Refernces