Technology Process of 3,5,7-Triacetoxy-4'-benzyloxy-flavon
There total 1 articles about 3,5,7-Triacetoxy-4'-benzyloxy-flavon which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2,4,6-Trihydroxy-ω-benzoyloxy-acetophenon 1.) 4-Benzoyloxy-benzoesaeureanhydrid 2.) KOH 3.) Acetanhydrid, Py.;
DOI:10.1002/cber.19701031131
- Guidance literature:
-
With
water; potassium carbonate; dimethyl sulfate;
In
acetone;
Heating;
1) 30 h; 2) 15 min;
DOI:10.1016/0040-4020(82)85113-2
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 64 percent / 1) Dimethylsulfat, K2CO3, 2) H2O / acetone / Heating; 1) 30 h; 2) 15 min
2: 29 percent / Sikkon, Ag2CO3 / various solvent(s) / 6 h / Ambient temperature
3: Pd/C / ethyl acetate / 3 h
4: NaOCH3 / methanol / Ambient temperature
With
Sikkon; water; sodium methylate; potassium carbonate; dimethyl sulfate; silver carbonate;
palladium on activated charcoal;
In
methanol; ethyl acetate; acetone;
DOI:10.1016/0040-4020(82)85113-2
