Technology Process of C42H54N6O11
There total 11 articles about C42H54N6O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 24h;
DOI:10.1021/ol902944f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / tetrahydrofuran / 2 h / -20 °C
1.2: 4 h / -20 - 20 °C
2.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h / -30 °C
2.2: 0.33 h / -30 - -20 °C
2.3: 8 h / -78 - 0 °C
3.1: sodium azide / N,N-dimethyl-formamide / 24 h / 20 °C
With
sodium azide; isopropylmagnesium chloride; triethylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2014.05.082
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dmap / acetonitrile
2.1: zinc; acetic acid / dichloromethane / 0.33 h / 0 - 20 °C
3.1: hydrogenchloride; sodium nitrite / tetrahydrofuran; water / 0.08 h / 0 °C
3.2: 1 h / 20 °C
4.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h / -30 °C
4.2: 0.33 h / -30 - -20 °C
4.3: 8 h / -78 - 0 °C
5.1: sodium azide / N,N-dimethyl-formamide / 24 h / 20 °C
With
hydrogenchloride; dmap; sodium azide; isopropylmagnesium chloride; acetic acid; zinc; sodium nitrite;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2014.05.082