lithium triisopropoxy phenyl borate

Base Information

• Chemical Name: lithium triisopropoxy phenyl borate
• CAS No.: 103885-19-4
• Molecular Formula: C₁₅H₂₆BO₃*Li
• Molecular Weight: 272.122
• Mol file: 103885-19-4.mol

Synonyms:lithium triisopropoxy phenyl borate

Chemical Property of lithium triisopropoxy phenyl borate

Chemical Property:

Purity/Quality:

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Technology Process of lithium triisopropoxy phenyl borate

There total 1 articles about lithium triisopropoxy phenyl borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromobenzene (108-86-1,52753-63-6) + Triisopropyl borate (5419-55-6) → lithium triisopropoxy phenyl borate (103885-19-4)

Guidance literature:

bromobenzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.25h;

Triisopropyl borate; In tetrahydrofuran; at -78 ℃; for 2h;

DOI:10.1016/j.cattod.2020.07.014

Reference yield:

lithium triisopropoxy phenyl borate (103885-19-4) + 4-iodobenzonitrile (3058-39-7) → 4-cyano-1,1'-biphenyl (2920-38-9)

Guidance literature:

In tetrahydrofuran; methanol; at 97 ℃; Temperature;

DOI:10.1016/j.cattod.2020.07.014

upstream raw materials:

bromobenzene

Triisopropyl borate

Downstream raw materials:

4-cyano-1,1'-biphenyl

Refernces