Technology Process of C38H38N10O2
There total 7 articles about C38H38N10O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; bathophenanthrolinedispufonic acid disodium salt; sodium L-ascorbate;
In
water; tert-butyl alcohol;
at 110 ℃;
for 0.25h;
Microwave irradiation;
DOI:10.1016/j.bmcl.2012.07.009
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; 2,6-dimethylpyridine / dichloromethane; tetrahydrofuran / 7.25 h / -78 - 0 °C / Molecular sieve; Inert atmosphere
2: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triphenylphosphine; piperidine / Molecular sieve; Inert atmosphere; Reflux
3: sodium hydroxide / tetrahydrofuran; water / 2 h / 20 °C
4: bathophenanthrolinedispufonic acid disodium salt; copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 0.25 h / 110 °C / Microwave irradiation
With
piperidine; 2,6-dimethylpyridine; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); copper(ll) sulfate pentahydrate; bathophenanthrolinedispufonic acid disodium salt; sodium L-ascorbate; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2012.07.009
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / tetrahydrofuran; water / 2 h / 20 °C
2: bathophenanthrolinedispufonic acid disodium salt; copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 0.25 h / 110 °C / Microwave irradiation
With
copper(ll) sulfate pentahydrate; bathophenanthrolinedispufonic acid disodium salt; sodium L-ascorbate; sodium hydroxide;
In
tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2012.07.009