3-Hydroxy-4-nitro-benzoylchlorid

Base Information

• Chemical Name: 3-Hydroxy-4-nitro-benzoylchlorid
• CAS No.: 36852-58-1
• Molecular Formula: C₇H₄ClNO₄
• Molecular Weight: 201.566
• Mol file: 36852-58-1.mol

Synonyms:3-Hydroxy-4-nitro-benzoylchlorid

Chemical Property of 3-Hydroxy-4-nitro-benzoylchlorid

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

3-Hydroxy-4-nitrobenzoyl chloride 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Hydroxy-4-nitro-benzoylchlorid

There total 2 articles about 3-Hydroxy-4-nitro-benzoylchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-hydroxy-4-nitro-benzoic acid (619-14-7) → 3-Hydroxy-4-nitro-benzoylchlorid (36852-58-1)

Guidance literature:

With thionyl chloride; iodine; Heating;

Reference yield:

→ 3-Hydroxy-4-nitro-benzoylchlorid (36852-58-1)

Guidance literature:

Reference yield:

3-Hydroxy-4-nitro-benzoylchlorid (36852-58-1) → 5-(hydroxymethyl)-2-nitrophenol (61161-83-9)

Guidance literature:

With sodium tetrahydroborate; In diethylene glycol dimethyl ether; at 60 - 70 ℃; for 3h; Yield given; other reagent: NaBH₄/AlCl₃;

upstream raw materials:

3-hydroxy-4-nitro-benzoic acid

Downstream raw materials:

5-(hydroxymethyl)-2-nitrophenol

C₁₅H₁₂N₂O₆

Refernces

• 1、 -. "Oxazinoquinolones useful for the treatment of viral infections". Page column 8. . Retrieved 2010/11/29.