Technology Process of C41H53N7O10S
There total 8 articles about C41H53N7O10S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 46.9 g / ammonium chloride / H2O; methanol / Heating
2.1: 2-methyl-propan-2-ol / 12 h / 20 °C
3.1: 21.9 g / H2; AcOH / PtO2 / 96 h / 35 °C
4.1: PyBop; diisopropylethylamine / dimethylformamide / 3.33 h / 0 - 20 °C
5.1: zinc; AcOH / 1.5 h / 20 °C
6.1: N-methylmorpholine; isobutyl chloroformate / dimethylformamide / 0.17 h / -15 °C
6.2: dimethylformamide / -15 - 20 °C
7.1: hydroxylamine*HCl; diisopropylethylamine / ethanol / Heating
8.1: AcOH / 20 °C
With
4-methyl-morpholine; hydroxylamine hydrochloride; ammonium chloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; isobutyl chloroformate;
platinum(IV) oxide;
In
methanol; ethanol; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm051272l
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 2-methyl-propan-2-ol / 12 h / 20 °C
2.1: 21.9 g / H2; AcOH / PtO2 / 96 h / 35 °C
3.1: PyBop; diisopropylethylamine / dimethylformamide / 3.33 h / 0 - 20 °C
4.1: zinc; AcOH / 1.5 h / 20 °C
5.1: N-methylmorpholine; isobutyl chloroformate / dimethylformamide / 0.17 h / -15 °C
5.2: dimethylformamide / -15 - 20 °C
6.1: hydroxylamine*HCl; diisopropylethylamine / ethanol / Heating
7.1: AcOH / 20 °C
With
4-methyl-morpholine; hydroxylamine hydrochloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; isobutyl chloroformate;
platinum(IV) oxide;
In
ethanol; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm051272l
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 21.9 g / H2; AcOH / PtO2 / 96 h / 35 °C
2.1: PyBop; diisopropylethylamine / dimethylformamide / 3.33 h / 0 - 20 °C
3.1: zinc; AcOH / 1.5 h / 20 °C
4.1: N-methylmorpholine; isobutyl chloroformate / dimethylformamide / 0.17 h / -15 °C
4.2: dimethylformamide / -15 - 20 °C
5.1: hydroxylamine*HCl; diisopropylethylamine / ethanol / Heating
6.1: AcOH / 20 °C
With
4-methyl-morpholine; hydroxylamine hydrochloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; isobutyl chloroformate;
platinum(IV) oxide;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm051272l