isolongifolan-10-one

Base Information

• Chemical Name: isolongifolan-10-one
• CAS No.: 41746-30-9
• Molecular Formula: C₁₅H₂₄O
• Molecular Weight: 220.355
• Mol file: 41746-30-9.mol

Synonyms:isolongifolan-10-one

Chemical Property of isolongifolan-10-one

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of isolongifolan-10-one

There total 6 articles about isolongifolan-10-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(-)-isolongifolene (1135-66-6) → 1,2,3,4,5,6-hexahydro-1,1,5,5-tetramethyl-7H-2,4a-methanonaphthalen-7-one (26839-52-1) + isolongifolan-10-one (41746-30-9) + Isolongifolene β-epoxide (26619-69-2,28370-55-0)

Guidance literature:

With oxygen; at 80 ℃; for 8h; under 7600.51 Torr; Pressure; Overall yield = 94 percent; Catalytic behavior; Mechanism; Green chemistry;

DOI:10.1016/j.ica.2020.120192

Reference yield:

→ 2,2,7,7-Tetramethyltricyclo<6.2.1.03.8>-undecan-4-on (23787-90-8,26839-48-5,26839-51-0,26839-72-5,29461-13-0,29461-14-1,41746-29-6,41746-30-9,57456-74-3,122743-47-9)

Guidance literature:

Keton IV (<α>(D): +9.2 grad), Filtration ueber akt. Al2O3;

DOI:10.1016/S0040-4020(01)97855-X

Reference yield:

→ (R)-1,1,5,5-Tetramethyl-hexahydro-2,4a-methano-naphthalen-8-one (23787-90-8,26839-48-5,26839-51-0,26839-72-5,29461-13-0,29461-14-1,41746-29-6,41746-30-9,57456-74-3,122743-47-9)

Guidance literature:

Verb. 1, BF3-katalys. Umlagerung;

DOI:10.1016/S0040-4039(01)98518-1

upstream raw materials:

(-)-isolongifolene

Refernces