17-Phenyl-2,9-dithia<1.10>paracyclophan

Base Information

• Chemical Name: 17-Phenyl-2,9-dithia<1.10>paracyclophan
• CAS No.: 82313-53-9
• Molecular Formula: C₂₇H₃₀S₂
• Molecular Weight: 418.667
• Mol file: 82313-53-9.mol

Synonyms:17-Phenyl-2,9-dithia<1.10>paracyclophan

Chemical Property of 17-Phenyl-2,9-dithia<1.10>paracyclophan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 17-Phenyl-2,9-dithia<1.10>paracyclophan

There total 1 articles about 17-Phenyl-2,9-dithia<1.10>paracyclophan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.5%

1,6-dimercaptohexane (1191-43-1) + 4,4'-Bis(brommethyl)triphenylmethan (82313-74-4) → 17-Phenyl-2,9-dithia<1.10>paracyclophan (82313-53-9)

Guidance literature:

With sodium hydroxide; In ethanol; toluene; Heating;

Reference yield: 80.0%

17-Phenyl-2,9-dithia<1.10>paracyclophan (82313-53-9) → 17-Phenyl-2,9-dithia<1.10>paracyclophan-2,2,9,9-tetraoxid (82324-74-1)

Guidance literature:

With dihydrogen peroxide; In acetic acid; at 20 ℃; for 24h;

Reference yield:

17-Phenyl-2,9-dithia<1.10>paracyclophan (82313-53-9) → 15-Phenyl<1.8>paracyclophan (82313-62-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / 60percent H₂O₂ / acetic acid / 24 h / 20 °C

2: 50 percent / 580 - 600 °C / 0.01 Torr

With dihydrogen peroxide; In acetic acid;

upstream raw materials:

1,6-dimercaptohexane

4,4'-Bis(brommethyl)triphenylmethan

Downstream raw materials:

17-Phenyl-2,9-dithia<1.10>paracyclophan-2,2,9,9-tetraoxid

15-Phenyl<1.8>paracyclophan

Refernces