Technology Process of C43H52F2N8O6Si
There total 11 articles about C43H52F2N8O6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C29H30F2N6Si;
With
N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.5h;
N-methoxycarbonyl-L-valine;
With
HATU;
In
N,N-dimethyl-formamide;
at -50 - 20 ℃;
for 14h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydroxide; sodium carbonate / water / 4 h / 0 - 20 °C
2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 0 °C
2.2: 14 h / -50 - 20 °C
With
sodium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 120 °C / Sealed tube
2.1: sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; 1,4-dioxane / 3 h / 85 °C / Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 0 °C
4.2: 14 h / -50 - 20 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium acetate; sodium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water; N,N-dimethyl-formamide;
